Ni-Ru supported on CeO2 obtained by mechanochemical milling for catalytic hydrogen production from ammonia

Developing active and stable catalysts for carbon-free hydrogen production is crucial to mitigate the effects of climate change. Ammonia is a promising carbon-free hydrogen source, as it has a high hydrogen content and is liquid at low pressure, which allows its easy storage and transportation. We h...

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Detalles Bibliográficos
Autores: Lucentini, Ilaria|||0000-0003-1311-9062, Serrano Carreño, M. Isabel|||0000-0002-4996-9280, García de Andrés, Xènia|||0000-0003-0795-4168, Garzón Manjón, Alba, Hu, Xinxin, Arbiol, Jordi, Pascua Solé, Laia|||0000-0001-9791-4586, Prat Albert, Jordi, Villalobos Portillo, Edgar Eduardo, Marini, Carlo, Escudero, Carlos, Llorca Piqué, Jordi|||0000-0002-7447-9582
Tipo de recurso: artículo
Fecha de publicación:2024
País:España
Institución:Universitat Politècnica de Catalunya (UPC)
Repositorio:UPCommons. Portal del coneixement obert de la UPC
Idioma:inglés
OAI Identifier:oai:upcommons.upc.edu:2117/413473
Acceso en línea:https://hdl.handle.net/2117/413473
https://dx.doi.org/10.1016/j.isci.2024.110028
Access Level:acceso abierto
Palabra clave:Catalysis
Energy application
Catàlisi
Àrees temàtiques de la UPC::Energies::Tecnologia energètica::Sistemes de transformació energètica
Descripción
Sumario:Developing active and stable catalysts for carbon-free hydrogen production is crucial to mitigate the effects of climate change. Ammonia is a promising carbon-free hydrogen source, as it has a high hydrogen content and is liquid at low pressure, which allows its easy storage and transportation. We have recently developed a nickel-based catalyst with a small content of ruthenium supported on cerium oxide, which exhibits high activity and stability in ammonia decomposition. Here, we investigate mechanochemical milling for its synthesis, a faster and less energy-consuming technique than conventional ones. Results indicate that mechanochemical synthesis increases catalytic activity compared to the conventional incipient wetness impregnation method. The interaction between the metal precursors and the support is key in fine-tuning catalytic activity, which increases linearly with oxygen vacancies in the support. Moreover, the mechanochemical method modifies the oxidation state of Ni and Ru species, with a variation depending on the precursors.