Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.

Dicksonia sellowiana Hook., Dicksoniaceae, is a tree-fern which is being recently used in medicine mainly for its phytotherapic activities. While several other studies have focused on D. sellowiana extract characterization in terms of its biological and antioxidant activity, the novelty of this work...

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Detalles Bibliográficos
Autores: MALUCELLI, L. C., MASSULO, T., MAGALHAES, W. L. E., STOFELLA, N. C. F., VASCONCELOS, E. C., CARVALHO FILHO, M. A. S., MURAKAMI, F. S.
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2018
País:Brasil
Institución:Empresa Brasileira de Pesquisa Agropecuária (Embrapa)
Repositorio:Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice)
Idioma:inglés
OAI Identifier:oai:www.alice.cnptia.embrapa.br:doc/1110898
Acceso en línea:http://www.alice.cnptia.embrapa.br/alice/handle/doc/1110898
Access Level:acceso abierto
Palabra clave:Thermal behavior pyrolysis
Thermal disposal
TG-MS
Pharmaceutical excipients
Pyrolisis
Spectometry
Compatibility
Pirólise
Espectometria
Termogravimetria
Dicksonia sellowiana
Thermogravimetry
Descripción
Sumario:Dicksonia sellowiana Hook., Dicksoniaceae, is a tree-fern which is being recently used in medicine mainly for its phytotherapic activities. While several other studies have focused on D. sellowiana extract characterization in terms of its biological and antioxidant activity, the novelty of this work aims to understand the fate of this extract during thermal disposal through thermogravimetry/differential thermal analysis, thermogravimetry/mass spectrometry, Fourier transform infrared spectroscopy and elemental analysis, to further characterize this plant?s extract. Thermal analysis revealed mass loss within three welldefined steps, with the respective mass signals represented generated during heating. Light-volatiles were released during the first step, with release of NO2, CO2, and ethanol in the following, as a result of extract pyrolytic decomposition. Furthermore, mass signals variation during heating indicated the release of harmless by products in contrast to other pharmaceutical and personal care products. Finally, chemical characterization confirmed the observed under thermal analysis suggesting a highly polar structure within extract?s composition.