Low temperature redetermination of the glycine sodium nitrate structure by using x-ray single crystal diffraction technique

The redetermined structure of glycine sodium nitrate, C2H5N2NaO5, at 150±K is reported. The compound has an overall polymeric structurewhilst the glycine molecule is found in the zwitterionic form. GSN crystals were characterized by XRD powder diffraction, FTIR, UV-VIS,and DTA-TGA techniques. XRD re...

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Detalhes bibliográficos
Autores: G.S. Nichol, J. Hernández Paredes, H.E Esparza Poncce, M. Pacheco Beltrán, M.E. Alvarez Ramos, A. Duarte-Moller
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2008
País:México
Recursos:Universidad de Sonora
Repositorio:Redalyc-USON
OAI Identifier:oai:redalyc.org:57054105
Acesso em linha:https://www.redalyc.org/articulo.oa?id=57054105
Access Level:acceso abierto
Palavra-chave:Física, Astronomía y Matemáticas
UV
XRD
Vis
FTIR
Polymers
Descrição
Resumo:The redetermined structure of glycine sodium nitrate, C2H5N2NaO5, at 150±K is reported. The compound has an overall polymeric structurewhilst the glycine molecule is found in the zwitterionic form. GSN crystals were characterized by XRD powder diffraction, FTIR, UV-VIS,and DTA-TGA techniques. XRD revealed that GSN have a monoclinic structure and space group Cc. Infrared spectra confirmed that thechemical elements and functional groups are present in the crystals and also collaborated the zwiterionic form of molecule. Ultraviolet-Visible spectra showed a wide optical transparent window in the range of 340-1100 nm, which is a desirable characteristic for nonlinearoptics applications. DTA-TGA analysis determined that the material is stable up to 198±C