Effect of BaCO3 reactivity and mixing procedure on sulfate-resistant cement performance

The present study focuses on exploring the effects of reactivity and degree of dispersion of BaCO additions in the manufacture of sulfate-resistant OPC cements. A new electrochemical deposition method is attempted to effectively disperse BaCO particles (studying two different materials with particle...

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Bibliographic Details
Authors: Carmona-Quiroga, Paula, Mota-Heredia, Carlos, Torres-Carrasco, Manuel, Fernández, José F., Blanco-Varela, María Teresa
Format: article
Status:Published version
Publication Date:2021
Country:España
Institution:Consejo Superior de Investigaciones Científicas (CSIC)
Repository:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/257646
Online Access:http://hdl.handle.net/10261/257646
Access Level:Open access
Keyword:Sulfate resistant cements
Cement paste
BaCO3
Electrodeposition
Fineness
Ettringite
Description
Summary:The present study focuses on exploring the effects of reactivity and degree of dispersion of BaCO additions in the manufacture of sulfate-resistant OPC cements. A new electrochemical deposition method is attempted to effectively disperse BaCO particles (studying two different materials with particle size: D = 11.45 and 2.37 μm) on cement to enhance their reactivity and favour sulfate immobilisation in the form of BaSO. The barium carbonate additions, particularly the finest, activate cement hydration to a greater extent. Electrodeposition is also observed to improve early age reactivity (2 d–7 d) in fine BaCO. Cement paste bearing 15 wt % BaCO is more resistant to sulfate attack by a 5% (w/v) solution of NaSO (180 d at 23 °C) than a commercial sulfate-resistant cement, although secondary ettringite and gypsum precipitated in all cases.