Novel Kazal-type proteinase inhibitors from the skin secretion of the Splendid leaf frog, Cruziohyla calcarifer

Peptidase inhibitors have an important role controlling a variety of biological processes. Here, we employed a peptidomic approach including molecular cloning, tandem mass spectrometry and enzymatic assays to reveal 7 Kazal-type proteinase inhibitors (CCKPs) (18 variants) in the skin secretion of th...

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Detalles Bibliográficos
Autores: Proaño Bolaños, Carolina, Li, Renjie, Zhou, Mei, Wang, Lei, Xi, Xinping, Tapia, Elicio E., Coloma, Luis A., Chen, Tianbao, Shaw, Chris
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2017
País:Ecuador
Institución:Universidad Regional Amazónica
Repositorio:Repositorio Universidad Regional Amazónica
OAI Identifier:oai:repositorio.ikiam.edu.ec:RD_IKIAM/130
Acceso en línea:https://doi.org/10.1016/j.euprot.2017.02.001
http://repositorio.ikiam.edu.ec/jspui/handle/RD_IKIAM/130
Access Level:acceso abierto
Palabra clave:Kazal-type proteinase inhibitors
Frog skin secretion
Peptidomic
Molecular cloning
Tandem mass spectrometry
Cruziohyla calcarifer
Descripción
Sumario:Peptidase inhibitors have an important role controlling a variety of biological processes. Here, we employed a peptidomic approach including molecular cloning, tandem mass spectrometry and enzymatic assays to reveal 7 Kazal-type proteinase inhibitors (CCKPs) (18 variants) in the skin secretion of the unexplored frog, Cruziohyla calcarifer. All 18 proteins shared the Kazal pattern C-X(7)-C-X(6,7)-C-X(6,7)-Y-X(3)-C-X(2)-C-X(15-21)-C and 3 disulphide bridges. Based on structural comparative analysis, we deemed trypsin and chymotrypsin inhibitory activity in CCKP-1, 4 and CCKP 2, 5, 7, respectively. These peptidase inhibitors presumably play a role to control the balance between other functional peptides produced in the amphibian skin secretions.