Synthesis of two new Nickel and CopperNickel vanadates used for propane oxidative dehydrogenation

ABSTRACT: Two new vanadates have been successfully synthesized by the hydrothermal and coprecipitation methods. Both vanadates were calcined at 600 °C and the resulting catalysts were tested on reaction of oxidative dehydrogenation of propane. The catalysts were characterized by x-ray diffraction, a...

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Detalhes bibliográficos
Autores: Hernández Naranjo, Juan Pablo, Echavarría, Adriana, Palacio Santos, Luz Amparo
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2013
País:Colombia
Recursos:Universidad de Antioquia
Repositorio:Repositorio UdeA
Idioma:inglés
OAI Identifier:oai:bibliotecadigital.udea.edu.co:10495/5441
Acesso em linha:http://hdl.handle.net/10495/5441
Access Level:acceso abierto
Palavra-chave:Vanadio
Níquel
Deshidrogenación
Descrição
Resumo:ABSTRACT: Two new vanadates have been successfully synthesized by the hydrothermal and coprecipitation methods. Both vanadates were calcined at 600 °C and the resulting catalysts were tested on reaction of oxidative dehydrogenation of propane. The catalysts were characterized by x-ray diffraction, atomic absorption, thermogravimetric analysis, and differential temperature analysis. The reaction was carried out in the temperature range of 350-500 °C. A conversion of propane of 10.6 % and a selectivity towards propene of 29.9 % at 400 °C were obtained with nickel vanadate; a conversion of 1.9 % and a selectivity of 56.9 % were reached at the same temperature with the nickel copper vanadate.