Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives

In the present communication, reported the easy, convenient route for the synthesis of N-formyl pyrazolines from α, β-unsaturated ketone. The aqueous 2-methoxyethanol was used as reaction media for the synthesis of titled compounds. All synthesized compounds were confirmed on the basis of IR,&nb...

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Detalles Bibliográficos
Autor: Zangade, Sainath
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2017
País:Brasil
Institución:Universidade Federal de Mato Grosso do Sul (UFMS)
Repositorio:Orbital - The Electronic Journal of Chemistry (Campo Grande)
Idioma:inglés
OAI Identifier:oai:periodicos.ufms.br:article/16458
Acceso en línea:https://periodicos.ufms.br/index.php/orbital/article/view/16458
Access Level:acceso abierto
Palabra clave:aqueous 2-methoxyethanol
hydrazine hydrate
irradiation of tungsten light
N-formyl-2-pyrazoline
α,β-unsaturated ketone
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spelling Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivativesaqueous 2-methoxyethanolhydrazine hydrateirradiation of tungsten lightN-formyl-2-pyrazolineα,β-unsaturated ketoneIn the present communication, reported the easy, convenient route for the synthesis of N-formyl pyrazolines from α, β-unsaturated ketone. The aqueous 2-methoxyethanol was used as reaction media for the synthesis of titled compounds. All synthesized compounds were confirmed on the basis of IR, 1H NMR, 13C NMR and CHN analysis. DOI: http://dx.doi.org/10.17807/orbital.v9i4.1010Instituto de Química, Universidade Federal de Mato Grosso do Sul2017-10-02info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionPeer-reviewedapplication/pdfapplication/pdfhttps://periodicos.ufms.br/index.php/orbital/article/view/16458Orbital: The Electronic Journal of Chemistry; Orbital - Vol. 9 No. 4 - July - September 2017; 315-317Orbital: The Electronic Journal of Chemistry; Orbital - Vol. 9 No. 4 - July - September 2017; 315-3171984-6428reponame:Orbital - The Electronic Journal of Chemistry (Campo Grande)instname:Universidade Federal de Mato Grosso do Sul (UFMS)instacron:UFMSenghttps://periodicos.ufms.br/index.php/orbital/article/view/16458/11150https://periodicos.ufms.br/index.php/orbital/article/view/16458/11151Copyright (c) 2017 Orbital: The Electronic Journal of Chemistryhttps://creativecommons.org/licenses/by-nc-nd/4.0info:eu-repo/semantics/openAccessZangade, Sainath2023-01-20T10:57:39Zoai:periodicos.ufms.br:article/16458Revistahttps://periodicos.ufms.br/index.php/orbital/indexPUBhttps://periodicos.ufms.br/index.php/orbital/oaieditor.orbital@ufms.br || marcos.amaral@ufms.br1984-64281984-6428opendoar:2023-01-20T10:57:39Orbital - The Electronic Journal of Chemistry (Campo Grande) - Universidade Federal de Mato Grosso do Sul (UFMS)false
dc.title.none.fl_str_mv Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives
title Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives
spellingShingle Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives
Zangade, Sainath
aqueous 2-methoxyethanol
hydrazine hydrate
irradiation of tungsten light
N-formyl-2-pyrazoline
α,β-unsaturated ketone
title_short Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives
title_full Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives
title_fullStr Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives
title_full_unstemmed Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives
title_sort Irradiation of Tungsten Light: A Useful Energy Source for Synthesis of 4,5-Dihydro-pyrazole-1-carbaldehyde Derivatives
dc.creator.none.fl_str_mv Zangade, Sainath
author Zangade, Sainath
author_facet Zangade, Sainath
author_role author
dc.subject.por.fl_str_mv aqueous 2-methoxyethanol
hydrazine hydrate
irradiation of tungsten light
N-formyl-2-pyrazoline
α,β-unsaturated ketone
topic aqueous 2-methoxyethanol
hydrazine hydrate
irradiation of tungsten light
N-formyl-2-pyrazoline
α,β-unsaturated ketone
description In the present communication, reported the easy, convenient route for the synthesis of N-formyl pyrazolines from α, β-unsaturated ketone. The aqueous 2-methoxyethanol was used as reaction media for the synthesis of titled compounds. All synthesized compounds were confirmed on the basis of IR, 1H NMR, 13C NMR and CHN analysis. DOI: http://dx.doi.org/10.17807/orbital.v9i4.1010
publishDate 2017
dc.date.none.fl_str_mv 2017-10-02
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
Peer-reviewed
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://periodicos.ufms.br/index.php/orbital/article/view/16458
url https://periodicos.ufms.br/index.php/orbital/article/view/16458
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv https://periodicos.ufms.br/index.php/orbital/article/view/16458/11150
https://periodicos.ufms.br/index.php/orbital/article/view/16458/11151
dc.rights.driver.fl_str_mv Copyright (c) 2017 Orbital: The Electronic Journal of Chemistry
https://creativecommons.org/licenses/by-nc-nd/4.0
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Copyright (c) 2017 Orbital: The Electronic Journal of Chemistry
https://creativecommons.org/licenses/by-nc-nd/4.0
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Instituto de Química, Universidade Federal de Mato Grosso do Sul
publisher.none.fl_str_mv Instituto de Química, Universidade Federal de Mato Grosso do Sul
dc.source.none.fl_str_mv Orbital: The Electronic Journal of Chemistry; Orbital - Vol. 9 No. 4 - July - September 2017; 315-317
Orbital: The Electronic Journal of Chemistry; Orbital - Vol. 9 No. 4 - July - September 2017; 315-317
1984-6428
reponame:Orbital - The Electronic Journal of Chemistry (Campo Grande)
instname:Universidade Federal de Mato Grosso do Sul (UFMS)
instacron:UFMS
instname_str Universidade Federal de Mato Grosso do Sul (UFMS)
instacron_str UFMS
institution UFMS
reponame_str Orbital - The Electronic Journal of Chemistry (Campo Grande)
collection Orbital - The Electronic Journal of Chemistry (Campo Grande)
repository.name.fl_str_mv Orbital - The Electronic Journal of Chemistry (Campo Grande) - Universidade Federal de Mato Grosso do Sul (UFMS)
repository.mail.fl_str_mv editor.orbital@ufms.br || marcos.amaral@ufms.br
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score 15.198674

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